Q11(a). Controlling supersaturation in gravimetry
Explain the general methods to avoid the supersaturation during precipitation in gravimetric estimation.
Answer in brief
Minimise local and relative supersaturation by slow precipitation from dilute, well-stirred solutions under conditions favouring crystal growth.
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Coversrelative supersaturationvon Weimarn rationucleationhomogeneous precipitationdigestiongravimetric analysis
All parts of Question 11
- 11(a) Controlling supersaturation in gravimetry10 marks
- 11(b) Peptisation and its prevention10 marks
- 11(c) Why excessive precipitant is avoided5 marks
- 11(d) Temperature and precipitate solubility5 marks