VKC ScienceChemistry for written exams Telegram

UPSC Combined Geo-Scientist

Chemist

  • 3 descriptive papers
  • 200 marks each
  • 3 h per paper

Mains Paper III covers analytical and organic chemistry.

UPSC Combined Geo-Scientist, Mains · 2019 · Mains Paper III

Q1(f). Proximate coal analysis

Question

Explain proximate analysis of coal.

Answer in brief

It determines moisture, volatile matter, ash and fixed carbon by specified heating and weighing procedures.

Key points

  • Dry a weighed sample near 105–110°C to determine moisture loss.
  • Heat a separate or sequential sample under prescribed covered/inert conditions at high temperature to determine volatile matter, correcting for moisture.
  • Burn the combustible material in air to constant residue to determine ash.
  • Fixed carbon is conventionally obtained by difference: 100-(%M+%VM+%ash) on the same reporting basis.
  • State whether results are as-received, dry or dry-ash-free; these are operational fractions, not a full elemental composition.

The full model answer

As written for the answer booklet: the diagram carries the working, the lines stay short. Read here only; it is not offered as a download.

Model answer to Q1(f), 2019 Mains Paper III: solution pages 3 and 4
Solution pages 3 and 4 of 19

CoversProximate coal analysisFuel analysis